SAE International Effect of SPS Process Parameters on the Densification Behaviour of Yttria Stabilized Zirconia 2014-01-0835

Description
Zirconium dioxide (ZrO 2 ) doped with Yttria exhibits superplastic behaviour, corrosion resistance and excellent ion conducting properties [ 1 ] at moderate temperatures and thus it can be used as an electroceramic to measure the pH of high temperature water used in fuel cells. Several fabrication processes are available for preparation of zirconia ceramics. This research focused on the study of using Spark Plasma Sintering (SPS) process to prepare Yttria Stabilized Zirconia (YSZ) ceramic. 8 mol% YSZ was subjected to varying SPS sintering conditions. Samples were sintered by changing the heating cycle, dwell time, sintering pressure and cooling cycle. Subsequently, these parameters were related to the densification characteristics of the as-sintered YSZ. The results of specific gravity measurements and microstructure evaluation suggest that stepped heating followed by a slow cooling results in YSZ with highest relative density (99.9%).
Description
Zirconium dioxide (ZrO 2 ) doped with Yttria exhibits superplastic behaviour, corrosion resistance and excellent ion conducting properties [ 1 ] at moderate temperatures and thus it can be used as an electroceramic to measure the pH of high temperature water used in fuel cells. Several fabrication processes are available for preparation of zirconia ceramics. This research focused on the study of using Spark Plasma Sintering (SPS) process to prepare Yttria Stabilized Zirconia (YSZ) ceramic. 8 mol% YSZ was subjected to varying SPS sintering conditions. Samples were sintered by changing the heating cycle, dwell time, sintering pressure and cooling cycle. Subsequently, these parameters were related to the densification characteristics of the as-sintered YSZ. The results of specific gravity measurements and microstructure evaluation suggest that stepped heating followed by a slow cooling results in YSZ with highest relative density (99.9%).

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Effect of SPS Process Parameters on the Densification Behaviour of Yttria Stabilized Zirconia - 2014-01-0835 - SAE International
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Effect of SPS Process Parameters on the Densification Behaviour of Yttria Stabilized Zirconia
2014-01-0835
Effect of SPS Process Parameters on the Densification Behaviour of Yttria Stabilized Zirconia 2014-01-0835
Zirconium dioxide (ZrO 2 ) doped with Yttria exhibits superplastic behaviour, corrosion resistance and excellent ion conducting properties [ 1 ] at moderate temperatures and thus it can be used as an electroceramic to measure the pH of high temperature water used in fuel cells. Several fabrication processes are available for preparation of zirconia ceramics. This research focused on the study of using Spark Plasma Sintering (SPS) process to prepare Yttria Stabilized Zirconia (YSZ) ceramic. 8 mol% YSZ was subjected to varying SPS sintering conditions. Samples were sintered by changing the heating cycle, dwell time, sintering pressure and cooling cycle. Subsequently, these parameters were related to the densification characteristics of the as-sintered YSZ. The results of specific gravity measurements and microstructure evaluation suggest that stepped heating followed by a slow cooling results in YSZ with highest relative density (99.9%).

Zirconium dioxide (ZrO 2 ) doped with Yttria exhibits superplastic behaviour, corrosion resistance and excellent ion conducting properties [ 1 ] at moderate temperatures and thus it can be used as an electroceramic to measure the pH of high temperature water used in fuel cells. Several fabrication processes are available for preparation of zirconia ceramics. This research focused on the study of using Spark Plasma Sintering (SPS) process to prepare Yttria Stabilized Zirconia (YSZ) ceramic. 8 mol% YSZ was subjected to varying SPS sintering conditions. Samples were sintered by changing the heating cycle, dwell time, sintering pressure and cooling cycle. Subsequently, these parameters were related to the densification characteristics of the as-sintered YSZ. The results of specific gravity measurements and microstructure evaluation suggest that stepped heating followed by a slow cooling results in YSZ with highest relative density (99.9%).

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  SAE International
Product Category Standards and Technical Documents
Product Number 2014-01-0835
Product Name Effect of SPS Process Parameters on the Densification Behaviour of Yttria Stabilized Zirconia
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