SIL6467.2 -- LITHIUM HEXAMETHYLDISILAZIDE, 0.85M IN HEXANE (19-21 WT %)
Gelest, Inc.LITHIUM HEXAMETHYLDISILAZIDE, 0.85M in hexane (19-21 wt %)SIL6467.2
Description
Additional Properties
Hydrolytic Sensitivity 7: reacts slowly with moisture/water Application Review of synthetic utility.1 Used in the use of chloroform in the trichloromethylation of a ketone in a scaled-up synthesis of ?-secretase inhibitor, spiropiperidine.2 Reference 1. Handbook of Reagents for Organic Synthesis, Reagents for Silicon-Mediated Organic Synthesis, Fuchs, P. L. Ed., John Wiley and Sons, Ltd., 2011, p. 356-367. 2. Henegar, K. E. et al. Org. Process. Res. Dev. 2013, 17, 985. Safety
Packaging Under Nitrogen
Gelest, Inc.
Done
Datasheet
Description
Additional Properties
Hydrolytic Sensitivity 7: reacts slowly with moisture/water Application Review of synthetic utility.1 Used in the use of chloroform in the trichloromethylation of a ketone in a scaled-up synthesis of ?-secretase inhibitor, spiropiperidine.2 Reference 1. Handbook of Reagents for Organic Synthesis, Reagents for Silicon-Mediated Organic Synthesis, Fuchs, P. L. Ed., John Wiley and Sons, Ltd., 2011, p. 356-367. 2. Henegar, K. E. et al. Org. Process. Res. Dev. 2013, 17, 985. Safety
Packaging Under Nitrogen
LITHIUM HEXAMETHYLDISILAZIDE, 0.85M in hexane (19-21 wt %)
SIL6467.2
LITHIUM HEXAMETHYLDISILAZIDE, 0.85M in hexane (19-21 wt %)
SIL6467.2
Additional Properties
Hydrolytic Sensitivity 7: reacts slowly with moisture/water Application Review of synthetic utility.1 Used in the use of chloroform in the trichloromethylation of a ketone in a scaled-up synthesis of ?-secretase inhibitor, spiropiperidine.2 Reference 1. Handbook of Reagents for Organic Synthesis, Reagents for Silicon-Mediated Organic Synthesis, Fuchs, P. L. Ed., John Wiley and Sons, Ltd., 2011, p. 356-367. 2. Henegar, K. E. et al. Org. Process. Res. Dev. 2013, 17, 985. Safety
Packaging Under Nitrogen
Additional Properties
Hydrolytic Sensitivity 7: reacts slowly with moisture/water
Application
Review of synthetic utility.1 Used in the use of chloroform in the trichloromethylation of a ketone in a scaled-up synthesis of ?-secretase inhibitor, spiropiperidine.2
Reference
1. Handbook of Reagents for Organic Synthesis, Reagents for Silicon-Mediated Organic Synthesis, Fuchs, P. L. Ed., John Wiley and Sons, Ltd., 2011, p. 356-367. 2. Henegar, K. E. et al. Org. Process. Res. Dev. 2013, 17, 985.
Safety
Packaging Under Nitrogen
Supplier's Site
Datasheet
Technical Specifications
Gelest, Inc.
Product Category
Inorganic Chemicals and Compounds
Product Number
SIL6467.2
Product Name
LITHIUM HEXAMETHYLDISILAZIDE, 0.85M in hexane (19-21 wt %)
